Information card for entry 4334041

Structure parameters

• Formula: C32 H56 N8 Ru2 Si4
• Calculated formula: C32 H56 N8 Ru2 Si4
• SMILES: c12cccc[n]1[RuH]134([Si](C)(N2C)C)([n]2c(cccc2)N(C)[Si]4(C)C)[H][RuH]243([n]3c(cccc3)N(C)[Si]2(C)C)([n]2c(cccc2)N(C)[Si]4(C)C)[H]1
• Title of publication: Step-by-Step Introduction of Silazane Moieties at Ruthenium: Different Extents of Ru-H-Si Bond Activation
• Authors of publication: Katharine A. Smart; Mary Grellier; Laure Vendier; Sax A. Mason; Silvia C. Capelli; Alberto Albinati; Sylviane Sabo-Etienne
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 2654 - 2661
• a: 12.536 ± 0.0002 Å
• b: 12.536 ± 0.0002 Å
• c: 12.8809 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2024.25 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 94
• Hermann-Mauguin space group symbol: P 42 21 2
• Hall space group symbol: P 4n 2n
• Residual factor for all reflections: 0.0188
• Residual factor for significantly intense reflections: 0.0156
• Weighted residual factors for significantly intense reflections: 0.0352
• Weighted residual factors for all reflections included in the refinement: 0.0356
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No