Information card for entry 4334051

Structure parameters

• Formula: C36 H56 Li N O2
• Calculated formula: C36 H56 Li N O2
• Title of publication: Structural Diversity in Alkali Metal Complexes of Sterically Demanding Carbazol-9-yl Ligands
• Authors of publication: Rhiannon S. Moorhouse; Graeme J. Moxey; Fabrizio Ortu; Thomas J. Reade; William Lewis; Alexander J. Blake; Deborah L. Kays
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 2678 - 2683
• a: 17.4299 ± 0.0018 Å
• b: 12.1842 ± 0.0013 Å
• c: 17.6287 ± 0.0018 Å
• α: 90°
• β: 113.07 ± 0.002°
• γ: 90°
• Cell volume: 3444.4 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.163
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.162
• Weighted residual factors for all reflections included in the refinement: 0.212
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No