Information card for entry 4334220

Structure parameters

• Chemical name: 2,2-bipyridine TEMPO nickel(II) hexafluorophosphate
• Formula: C19.5 H27 Cl F6 N3 Ni O P
• Calculated formula: C19.5 H27 Cl F6 N3 Ni O P
• Title of publication: Nitric Oxide Release from a Nickel Nitrosyl Complex Induced by One-Electron Oxidation
• Authors of publication: Ashley M. Wright; Homaira T. Zaman; Guang Wu; Trevor W. Hayton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 3207 - 3216
• a: 21.24 ± 0.007 Å
• b: 9.737 ± 0.003 Å
• c: 22.745 ± 0.008 Å
• α: 90°
• β: 90.718 ± 0.006°
• γ: 90°
• Cell volume: 4704 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0297
• Weighted residual factors for significantly intense reflections: 0.0598
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No