Information card for entry 4334621

Structure parameters

• Chemical name: tris(μ2-1,3-bis(4,4,4-Trifluoro-3-oxido-1-(oxo)but-2-en-1-yl)phenyl)- bis(1,2-dimethoxyethane-O,O')-di-Samarium(iii)
• Formula: C50 H38 F18 O16 Sm2
• Calculated formula: C50 H38 F18 O16 Sm2
• Title of publication: Crystal Structure and Highly Luminescent Properties Studies of Bis-β-diketonate Lanthanide Complexes
• Authors of publication: Jing Shi; Yanjun Hou; Wenyi Chu; Xiaohong Shi; Huiquan Gu; Bilin Wang; Zhizhong Sun
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5013 - 5022
• a: 15.6073 ± 0.0008 Å
• b: 12.9464 ± 0.0006 Å
• c: 29.3024 ± 0.0014 Å
• α: 90°
• β: 92.016 ± 0.001°
• γ: 90°
• Cell volume: 5917.1 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0332
• Residual factor for significantly intense reflections: 0.0297
• Weighted residual factors for significantly intense reflections: 0.0656
• Weighted residual factors for all reflections included in the refinement: 0.0672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.159
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No