Information card for entry 4334748

Structure parameters

• Formula: C28 H48 Ni O2 P2
• Calculated formula: C28 H48 Ni O2 P2
• Title of publication: Synthesis of New Late Transition Metal P,P-, P,N-, and P,O- Complexes Using Phosphonium Dimers as Convenient Ligand Precursors
• Authors of publication: Kanghee Park; Paraskevi O. Lagaditis; Alan J. Lough; Robert H. Morris
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5448 - 5456
• a: 9.8176 ± 0.0007 Å
• b: 11.9293 ± 0.0007 Å
• c: 14.3536 ± 0.001 Å
• α: 97.088 ± 0.003°
• β: 109.224 ± 0.003°
• γ: 114.046 ± 0.003°
• Cell volume: 1383.39 ± 0.17 ų
• Cell temperature: 147 ± 1 K
• Ambient diffraction temperature: 147 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0918
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1463
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No