Crystallography Open Database

Information card for entry 4334855

Preview

Coordinates	4334855.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H64 F24 P8 Pt2 S4
Calculated formula	C68 H64 F24 P8 Pt2 S4
Title of publication	General Strategy for the Synthesis of Rigid Weak-Link Approach Platinum(II) Complexes: Tweezers, Triple-Layer Complexes, and Macrocycles
Authors of publication	Robert D. Kennedy; Charles W. Machan; C. Michael McGuirk; Mari S. Rosen; Charlotte L. Stern; Amy A. Sarjeant; Chad A. Mirkin
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	5876 - 5888
a	20.2651 ± 0.0005 Å
b	20.2651 ± 0.0005 Å
c	43.292 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	17778.9 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	88
Hermann-Mauguin space group symbol	I 41/a :2
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.1299
Residual factor for significantly intense reflections	0.097
Weighted residual factors for significantly intense reflections	0.2577
Weighted residual factors for all reflections included in the refinement	0.2814
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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