Information card for entry 4335207

Structure parameters

• Formula: C78.5 H60.5 N8.5 O4 U
• Calculated formula: C78.5 H60.5 N8.5 O4 U
• Title of publication: Synthesis of Electron-Rich Uranium(IV) Complexes Supported by Tridentate Schiff Base Ligands and Their Multi-Electron Redox Chemistry
• Authors of publication: Clément Camp; Julie Andrez; Jacques Pécaut; Marinella Mazzanti
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7078 - 7086
• a: 45.625 ± 0.002 Å
• b: 15.8387 ± 0.0009 Å
• c: 18.5959 ± 0.0013 Å
• α: 90°
• β: 110.506 ± 0.005°
• γ: 90°
• Cell volume: 12586.7 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1181
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1318
• Weighted residual factors for all reflections included in the refinement: 0.1654
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No