Information card for entry 4335254

Structure parameters

• Formula: C27 H36 Ge N8
• Calculated formula: C27 H36 Ge N8
• Title of publication: Synthesis and Structure of Base-Stabilized Germanium(II) Diazide IPrGe(N3)2
• Authors of publication: Benjamin Lyhs; Dieter Bläser; Christoph Wölper; Stephan Schulz; Rebekka Haack; Georg Jansen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7236 - 7241
• a: 16.5337 ± 0.0003 Å
• b: 9.4188 ± 0.0002 Å
• c: 17.794 ± 0.0004 Å
• α: 90°
• β: 90.631 ± 0.001°
• γ: 90°
• Cell volume: 2770.85 ± 0.1 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0551
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.1095
• Weighted residual factors for all reflections included in the refinement: 0.1168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No