Information card for entry 4335360

Structure parameters

• Formula: C48 H86 N6 O15 P2 Pd6
• Calculated formula: C48 H84 N6 O15 P2 Pd6
• Title of publication: Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
• Authors of publication: Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7608 - 7614
• a: 15.31 ± 0.002 Å
• b: 21.694 ± 0.002 Å
• c: 19.245 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6391.9 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.1158
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for significantly intense reflections: 0.1135
• Weighted residual factors for all reflections included in the refinement: 0.1338
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No