Information card for entry 4335428

Structure parameters

• Common name: DMF@[Ag4(tppepb)4]I4
• Formula: C276 H208.48 Ag4 I4 N4 O4 P12
• Calculated formula: C276 H208.48 Ag4 I4 N4 O4 P12
• Title of publication: Self-Assembled Supramolecular Clusters Based on Phosphines and Coinage Metals: Tetrahedra, Helicates, and Mesocates
• Authors of publication: Sang Ho Lim; Seth M. Cohen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7862 - 7872
• a: 69.8512 ± 0.0018 Å
• b: 19.7868 ± 0.0005 Å
• c: 38.2622 ± 0.0011 Å
• α: 90°
• β: 92.882 ± 0.002°
• γ: 90°
• Cell volume: 52817 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.0814
• Weighted residual factors for significantly intense reflections: 0.2373
• Weighted residual factors for all reflections included in the refinement: 0.2485
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No