Information card for entry 4335492

Structure parameters

• Common name: (ONO)ReO(PPh3)
• Chemical name: Oxo(triphenylphosphine)(bis(3,5-di-tert-butyl-2-phenoxo)amido)rhenium(V)
• Formula: C46 H55 N O3 P Re
• Calculated formula: C46 H55 N O3 P Re
• Title of publication: Nonclassical Oxygen Atom Transfer as a Synthetic Strategy: Preparation of an Oxorhenium(V) Complex of the Bis(3,5-di-tert-butyl-2-phenoxo)amide Ligand
• Authors of publication: Daniel D. Wright; Seth N. Brown
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 7831 - 7833
• a: 10.162 ± 0.0006 Å
• b: 14.7652 ± 0.0009 Å
• c: 28.6116 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4293 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.024
• Residual factor for significantly intense reflections: 0.0204
• Weighted residual factors for significantly intense reflections: 0.0381
• Weighted residual factors for all reflections included in the refinement: 0.0387
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No