Information card for entry 4335546

Structure parameters

• Formula: C96 Co4 N6 O80 Si2 W20
• Calculated formula: C96 Co4 N6 O80 Si2 W20
• Title of publication: Synthesis, Structure Characterization, and Reversible Transformation of a Cobalt Salt of a Dilacunary γ-Keggin Silicotungstate and Sandwich-Type Di- and Tetracobalt-Containing Silicotungstate Dimers
• Authors of publication: Yuji Kikukawa; Kosuke Suzuki; Kazuya Yamaguchi; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 8644 - 8652
• a: 25.4252 ± 0.0004 Å
• b: 24.6889 ± 0.0004 Å
• c: 28.3278 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 17781.9 ± 0.5 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.098
• Weighted residual factors for all reflections included in the refinement: 0.2793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No