Crystallography Open Database

Information card for entry 4335725

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Coordinates	4335725.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H46 N4 O4
Calculated formula	C34 H46 N4 O4
Title of publication	Aryl-Linked Salicylaldoxime-Based Copper(II) Helicates and "Boxes": Synthesis, X-ray Analysis, and Anion Influence on Complex Structure
Authors of publication	Ajay Pal Singh Pannu; James R. Stevens; Paul G. Plieger
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	9327 - 9337
a	25.7501 ± 0.0009 Å
b	8.7686 ± 0.0003 Å
c	14.9082 ± 0.0012 Å
α	90°
β	113.157 ± 0.017°
γ	90°
Cell volume	3094.9 ± 0.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1367
Residual factor for significantly intense reflections	0.0799
Weighted residual factors for significantly intense reflections	0.2075
Weighted residual factors for all reflections included in the refinement	0.2603
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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