Information card for entry 4335813

Structure parameters

• Formula: C84 H132 P4 Ru2 Si4
• Calculated formula: C84 H132 P4 Ru2 Si4
• Title of publication: Phosphinodi(benzylsilane) PhP{(o-C6H4CH2)SiMe2H}2: A Versatile "PSi2Hx" Pincer-Type Ligand at Ruthenium
• Authors of publication: Virginia Montiel-Palma; Miguel A. Muñoz-Hernández; Cynthia A. Cuevas-Chávez; Laure Vendier; Mary Grellier; Sylviane Sabo-Etienne
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 9798 - 9806
• a: 37.6275 ± 0.0015 Å
• b: 10.4778 ± 0.0003 Å
• c: 20.726 ± 0.005 Å
• α: 90°
• β: 97.93 ± 0.003°
• γ: 90°
• Cell volume: 8093 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0998
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.0947
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No