Information card for entry 4335866

Structure parameters

• Formula: C40 H46 Dy6 F24 N4 O36 P12 S16
• Calculated formula: C40 H46 Dy6 F24 N4 O36 P12 S16
• Title of publication: Difluorodioxophosphate-Based Hollow Hexanuclear Lanthanide(III) Clusters Decorated with Tetrathiafulvalene Ligands
• Authors of publication: Tamyris T. da Cunha; Fabrice Pointillart; Boris Le Guennic; Cynthia L. M. Pereira; Stéphane Golhen; Olivier Cador; Lahcène Ouahab
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 9711 - 9713
• a: 35.874 ± 0.001 Å
• b: 26.481 ± 0.001 Å
• c: 14.684 ± 0.001 Å
• α: 90°
• β: 100.879 ± 0.01°
• γ: 90°
• Cell volume: 13698.8 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1003
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.1364
• Weighted residual factors for all reflections included in the refinement: 0.1529
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No