Information card for entry 4335906

Structure parameters

• Formula: C40.5 H37 F8 N7 Zr
• Calculated formula: C40.5 H37 F8 N7 Zr
• Title of publication: Zirconium Complexes Supported by an N-Perfluoro-Arylated Diamidopyridyl Ligand: Synthesis of Hydrazinediido Complexes
• Authors of publication: Solveig A. Scholl; Gudrun T. Plundrich; Hubert Wadepohl; Lutz H. Gade
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 10158 - 10166
• a: 11.2275 ± 0.0002 Å
• b: 13.765 ± 0.0003 Å
• c: 14.1485 ± 0.0003 Å
• α: 112.625 ± 0.002°
• β: 105.15 ± 0.0018°
• γ: 101.223 ± 0.0018°
• Cell volume: 1838.16 ± 0.08 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0271
• Residual factor for significantly intense reflections: 0.0245
• Weighted residual factors for significantly intense reflections: 0.0588
• Weighted residual factors for all reflections included in the refinement: 0.0599
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No