Information card for entry 4336063

Structure parameters

• Formula: C6.75 K4 N6 O0.25 S6 V
• Calculated formula: C11.6568 K4 N6 Ni S6
• Title of publication: First Row Transition Metal(II) Thiocyanate Complexes, and Formation of 1-, 2-, and 3-Dimensional Extended Network Structures of M(NCS)2(Solvent)2 (M = Cr, Mn, Co) Composition
• Authors of publication: Endrit Shurdha; Curtis E. Moore; Arnold L. Rheingold; Saul H. Lapidus; Peter W. Stephens; Atta M. Arif; Joel S. Miller
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 10583 - 10594
• a: 8.451111 ± 0.000078 Å
• b: 8.451111 Å
• c: 9.16677 ± 0.00017 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 566.989 ± 0.012 ų
• Cell temperature: 295 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 193
• Hermann-Mauguin space group symbol: P 63/m c m
• Hall space group symbol: -P 6c 2
• Goodness-of-fit parameter for all reflections: 3.549
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 0.699974 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes