Information card for entry 4336287

Structure parameters

• Chemical name: N-[2,6-bis(2,4,6-trimethylphenyl)phenyl]-N-(trimethylsilyl)amino- dichlorophosphane
• Formula: C27 H34 Cl2 N P Si
• Calculated formula: C27 H34 Cl2 N P Si
• SMILES: P(Cl)(Cl)N([Si](C)(C)C)c1c(c2c(C)cc(cc2C)C)cccc1c1c(cc(cc1C)C)C
• Title of publication: Synthesis of 1,3-Dichloro-cyclo-1,3-diphosphadiazanes from Silylated Amino(dichloro)phosphanes
• Authors of publication: Axel Schulz; Alexander Villinger; Andrea Westenkirchner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11457 - 11468
• a: 16.1703 ± 0.0005 Å
• b: 17.8854 ± 0.0005 Å
• c: 18.311 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5295.8 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0949
• Weighted residual factors for all reflections included in the refinement: 0.1082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No