Information card for entry 4336293

Structure parameters

• Chemical name: 1,3-dichloro-2,4-bis(2,6-bis(2,4,6-trimethylphenyl)phenyl)-cyclo-1,3- diphospha-2,4-diazane
• Formula: C48 H50 Cl2 N2 P2
• Calculated formula: C48 H50 Cl2 N2 P2
• Title of publication: Synthesis of 1,3-Dichloro-cyclo-1,3-diphosphadiazanes from Silylated Amino(dichloro)phosphanes
• Authors of publication: Axel Schulz; Alexander Villinger; Andrea Westenkirchner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11457 - 11468
• a: 21.9363 ± 0.0016 Å
• b: 44.948 ± 0.003 Å
• c: 8.5007 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8381.6 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1386
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No