Information card for entry 4336296

Structure parameters

• Chemical name: 1,3-dichloro-2,4-bis(triphenylmethyl)-cyclo-1,3-diphospha-2,4-diazane dichloromethane solvate
• Formula: C39 H32 Cl4 N2 P2
• Calculated formula: C39 H32 Cl4 N2 P2
• Title of publication: Synthesis of 1,3-Dichloro-cyclo-1,3-diphosphadiazanes from Silylated Amino(dichloro)phosphanes
• Authors of publication: Axel Schulz; Alexander Villinger; Andrea Westenkirchner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11457 - 11468
• a: 9.915 ± 0.0003 Å
• b: 14.6355 ± 0.0004 Å
• c: 12.0346 ± 0.0003 Å
• α: 90°
• β: 90.437 ± 0.002°
• γ: 90°
• Cell volume: 1746.3 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0636
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No