Information card for entry 4336318

Structure parameters

• Formula: C33 H56 N4 Si Ti3
• Calculated formula: C33 H56 N4 Si Ti3
• Title of publication: Reactivity with Electrophiles of Imido Groups Supported on Trinuclear Titanium Systems
• Authors of publication: Jorge Caballo; Mariano González-Moreiras; Miguel Mena; Adrián Pérez-Redondo; Carlos Yélamos
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11519 - 11529
• a: 11.293 ± 0.006 Å
• b: 12.6914 ± 0.0013 Å
• c: 12.788 ± 0.007 Å
• α: 95.11 ± 0.03°
• β: 100.16 ± 0.03°
• γ: 98.3 ± 0.03°
• Cell volume: 1772.8 ± 1.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0828
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1356
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No