Information card for entry 4336410

Structure parameters

• Formula: C29 H60 Cl4 N10 Ni3 O20
• Calculated formula: C29 H60 Cl4 N10 Ni3 O20
• Title of publication: Di-, Tri-, and Tetranuclear Nickel(II) Complexes with Oximato Bridges: Magnetism and Catecholase-like Activity of Two Tetranuclear Complexes Possessing Rhombic Topology
• Authors of publication: Lakshmi Kanta Das; Apurba Biswas; Jared S. Kinyon; Naresh S. Dalal; Haidong Zhou; Ashutosh Ghosh
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11744 - 11757
• a: 12.2018 ± 0.0003 Å
• b: 14.4627 ± 0.0004 Å
• c: 16.0305 ± 0.0007 Å
• α: 105.075 ± 0.002°
• β: 95.379 ± 0.002°
• γ: 113.578 ± 0.001°
• Cell volume: 2440.2 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0963
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for significantly intense reflections: 0.19
• Weighted residual factors for all reflections included in the refinement: 0.22
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No