Information card for entry 4336431

Structure parameters

• Formula: C67.84 H65.68 Cl4 Fe P4 Pd
• Calculated formula: C67.84 H65.68 Cl4 Fe P4 Pd
• Title of publication: Kinetic and Electrochemical Studies of the Oxidative Addition of Demanding Organic Halides to Pd(0): the Efficiency of Polyphosphane Ligands in Low Palladium Loading Cross-Couplings Decrypted
• Authors of publication: Veronika A. Zinovyeva; Sophal Mom; Sophie Fournier; Charles H. Devillers; Hélène Cattey; Henri Doucet; Jean-Cyrille Hierso; Dominique Lucas
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 11923 - 11933
• a: 14.3917 ± 0.0004 Å
• b: 20.0428 ± 0.0006 Å
• c: 25.2108 ± 0.0006 Å
• α: 90°
• β: 120.253 ± 0.001°
• γ: 90°
• Cell volume: 6281.7 ± 0.3 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0631
• Weighted residual factors for significantly intense reflections: 0.1399
• Weighted residual factors for all reflections included in the refinement: 0.1424
• Goodness-of-fit parameter for all reflections included in the refinement: 1.196
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No