Information card for entry 4336460

Structure parameters

• Formula: C42.5 H56 Cl O P2 Rh Si
• Calculated formula: C42.5 H56 Cl O P2 Rh Si
• Title of publication: POP-Pincer Silyl Complexes of Group 9: Rhodium versus Iridium
• Authors of publication: Miguel A. Esteruelas; Montserrat Oliván; Andrea Vélez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 12108 - 12119
• a: 31.6766 ± 0.0018 Å
• b: 11.6863 ± 0.0007 Å
• c: 22.6325 ± 0.0013 Å
• α: 90°
• β: 107.206 ± 0.001°
• γ: 90°
• Cell volume: 8003.2 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1203
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No