Crystallography Open Database

Information card for entry 4336462

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Coordinates	4336462.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H62 Cl O P2 Rh Si
Calculated formula	C51 H62 Cl O P2 Rh Si
Title of publication	POP-Pincer Silyl Complexes of Group 9: Rhodium versus Iridium
Authors of publication	Miguel A. Esteruelas; Montserrat Oliván; Andrea Vélez
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	12108 - 12119
a	10.2599 ± 0.0007 Å
b	11.9553 ± 0.0008 Å
c	20.3304 ± 0.0014 Å
α	77.896 ± 0.001°
β	84.276 ± 0.001°
γ	71.924 ± 0.001°
Cell volume	2316.3 ± 0.3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0611
Residual factor for significantly intense reflections	0.046
Weighted residual factors for significantly intense reflections	0.0873
Weighted residual factors for all reflections included in the refinement	0.094
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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