Information card for entry 4337010

Structure parameters

• Formula: C130 H213 Ga6 N14 Ni8
• Calculated formula: C130 H213 Ga6 N14 Ni8
• Title of publication: Clusters [Ma(GaCp*)b(CNR)c] (M = Ni, Pd, Pt): Synthesis, Structure, and Ga/Zn Exchange Reactions
• Authors of publication: Mariusz Molon; Katharina Dilchert; Christian Gemel; Rüdiger W. Seidel; Julian Schaumann; Roland A. Fischer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 14275 - 14283
• a: 14.9307 ± 0.0004 Å
• b: 22.7367 ± 0.0006 Å
• c: 24.1929 ± 0.0006 Å
• α: 73.638 ± 0.002°
• β: 88.638 ± 0.002°
• γ: 71.327 ± 0.002°
• Cell volume: 7445.5 ± 0.4 ų
• Cell temperature: 105 ± 2 K
• Ambient diffraction temperature: 105 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1149
• Weighted residual factors for all reflections included in the refinement: 0.1272
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No