Information card for entry 4337117

Structure parameters

• Formula: Bi2 H10.07 K1.7 Mo9.4 O45.03 V3.6
• Calculated formula: Bi2 H9.924 K1.777 Mo9.36 O44.962 V3.64
• Title of publication: Tetrahedral Connection of ε-Keggin-type Polyoxometalates To Form an All-Inorganic Octahedral Molecular Sieve with an Intrinsic 3D Pore System.
• Authors of publication: Zhang, Zhenxin; Sadakane, Masahiro; Murayama, Toru; Izumi, Shoko; Yasuda, Nobuhiro; Sakaguchi, Norihito; Ueda, Wataru
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 2
• Pages of publication: 903 - 911
• a: 19.685 ± 0.0006 Å
• b: 19.685 ± 0.0006 Å
• c: 19.685 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7627.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 227
• Hermann-Mauguin space group symbol: F d -3 m :2
• Hall space group symbol: -F 4vw 2vw 3
• Residual factor for all reflections: 0.0579
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0616
• Weighted residual factors for all reflections included in the refinement: 0.0646
• Goodness-of-fit parameter for all reflections included in the refinement: 0.904
• Diffraction radiation wavelength: 0.83112 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No