Information card for entry 4337171

Structure parameters

• Formula: C24 H64 B4 Ca N2 O9
• Calculated formula: C24 H64 B4 Ca N2 O9
• Title of publication: Synthesis and characterization of calcium n,n-dimethylaminodiboranates as possible chemical vapor deposition precursors.
• Authors of publication: Dunbar, Andrew C.; Girolami, Gregory S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 2
• Pages of publication: 888 - 896
• a: 15.7631 ± 0.001 Å
• b: 10.1952 ± 0.0006 Å
• c: 23.2794 ± 0.0015 Å
• α: 90°
• β: 104.528 ± 0.003°
• γ: 90°
• Cell volume: 3621.6 ± 0.4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0885
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1243
• Goodness-of-fit parameter for all reflections included in the refinement: 0.91
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No