Dinuclear Metallacycles with Single M-O(H)-M Bridges [M = Fe(II), Co(II), Ni(II), Cu(II)]: Effects of Large Bridging Angles on Structure and Antiferromagnetic Superexchange Interactions.
Authors of publication
Reger, Daniel L.; Pascui, Andrea E.; Foley, Elizabeth A.; Smith, Mark D.; Jezierska, Julia; Ozarowski, Andrew
Journal of publication
Inorganic chemistry
Year of publication
2014
Journal volume
53
Journal issue
4
Pages of publication
1975 - 1988
a
11.6805 ± 0.0005 Å
b
14.072 ± 0.0006 Å
c
15.4802 ± 0.0006 Å
α
93.721 ± 0.001°
β
103.333 ± 0.001°
γ
101.286 ± 0.001°
Cell volume
2411.79 ± 0.17 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0502
Residual factor for significantly intense reflections
0.0411
Weighted residual factors for significantly intense reflections
0.1043
Weighted residual factors for all reflections included in the refinement
0.1102
Goodness-of-fit parameter for all reflections included in the refinement
