Information card for entry 4337351

Structure parameters

• Formula: C12 H16 Cl3 N2 O2 Os
• Calculated formula: C12 H16 Cl3 N2 O2 Os
• SMILES: [Os]1(Cl)(Cl)(Cl)([OH]C)[n]2ccccc2c2[n]1cccc2.OC
• Title of publication: Solvent-Dependent Formation of Os(0) Complexes by Electrochemical Reduction of [Os(CO)(2,2'-bipyridine)(L)Cl2]; L = Cl(-), PrCN.
• Authors of publication: Tory, Joanne; King, Lisa; Maroulis, Antonios; Haukka, Matti; Calhorda, Maria José; Hartl, František
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1382 - 1396
• a: 6.5802 ± 0.0003 Å
• b: 14.2081 ± 0.0014 Å
• c: 16.4891 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1541.6 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0205
• Residual factor for significantly intense reflections: 0.0168
• Weighted residual factors for significantly intense reflections: 0.0284
• Weighted residual factors for all reflections included in the refinement: 0.0292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No