Information card for entry 4337387

Structure parameters

• Chemical name: bis(μ~3~-1,2-dithiolatoethane-S,S,S',S')-tetra(vinylido) -bis(triisopropylphosphine)-dicopper(+1)-dialuminium(+3)
• Formula: C30 H62 Al2 Cu2 P2 S4
• Calculated formula: C30 H62 Al2 Cu2 P2 S4
• Title of publication: Trialkylphosphine-Stabilized Copper(I) Dialkylaluminum(III) Ethanedithiolate Complexes: Single-Source Precursors and a Novel Modification of Copper Aluminum Disulfide.
• Authors of publication: Kischel, Marcus; Dornberg, Gregor; Krautscheid, Harald
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1614 - 1623
• a: 10.6765 ± 0.0008 Å
• b: 16.4983 ± 0.001 Å
• c: 11.7204 ± 0.0009 Å
• α: 90°
• β: 95.986 ± 0.006°
• γ: 90°
• Cell volume: 2053.2 ± 0.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0783
• Weighted residual factors for all reflections included in the refinement: 0.0803
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No