Information card for entry 4337399

Structure parameters

• Chemical name: Bis((2,4,6,2'',4'',6''-hexamethyl-1,1':3';1''-terphenyl- 2')amido)tetramethyldisilazanido-N,N',N"-praseodymium tris(tetrahydrofuran)solvate
• Formula: C60 H78 N3 O2 Pr Si2
• Calculated formula: C60 H78 N3 O2 Pr Si2
• Title of publication: Formation of Novel T-Shaped NNN Ligands via Rare-Earth Metal-Mediated Si-H Activation.
• Authors of publication: Bubrin, Denis; Niemeyer, Mark
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1269 - 1271
• a: 13.8928 ± 0.0006 Å
• b: 15.3039 ± 0.0006 Å
• c: 15.7594 ± 0.0006 Å
• α: 80.973 ± 0.002°
• β: 83.157 ± 0.002°
• γ: 63.777 ± 0.002°
• Cell volume: 2963.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0558
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1063
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.431
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No