Information card for entry 4337401

Structure parameters

• Chemical name: Tris(tetramethyldisilazanido)bis(tetrahydrofuran)cerium
• Formula: C20 H58 Ce N3 O2 Si6
• Calculated formula: C20 H58 Ce N3 O2 Si6
• Title of publication: Formation of Novel T-Shaped NNN Ligands via Rare-Earth Metal-Mediated Si-H Activation.
• Authors of publication: Bubrin, Denis; Niemeyer, Mark
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1269 - 1271
• a: 13.232 ± 0.003 Å
• b: 16.457 ± 0.004 Å
• c: 16.928 ± 0.003 Å
• α: 90°
• β: 91.144 ± 0.016°
• γ: 90°
• Cell volume: 3685.5 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1058
• Weighted residual factors for all reflections included in the refinement: 0.1089
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No