Information card for entry 4337407

Structure parameters

• Formula: C46 H81 N2 O3 Si2 Yb
• Calculated formula: C46 H81 N2 O3 Si2 Yb
• Title of publication: Divalent heteroleptic ytterbium complexes - effective catalysts for intermolecular styrene hydrophosphination and hydroamination.
• Authors of publication: Basalov, Ivan V.; Roşca, Sorin Claudiu; Lyubov, Dmitry M.; Selikhov, Alexander N.; Fukin, Georgy K.; Sarazin, Yann; Carpentier, Jean-François; Trifonov, Alexander A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1654 - 1661
• a: 18.6631 ± 0.0014 Å
• b: 24.0308 ± 0.0018 Å
• c: 10.9921 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4929.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0733
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.0787
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No