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Information card for entry 4337415
Preview
Coordinates | 4337415.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C152 H145 N O34.5 P3 W4 |
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Calculated formula | C150.761 H125.943 N O34.381 P3 W4 |
Title of publication | Synthesis, Structure and Cation-Binding Properties of Some [4 + 4] Metallocyclic MO2(2+) (M = Mo or W) Derivatives of 9-Phenyl-2,3,7-trihydroxyfluor-6-one. |
Authors of publication | McCormick, Laura J.; Abrahams, Brendan F.; Boughton, Berin A.; Grannas, Martin J.; Hudson, Timothy A.; Robson, Richard |
Journal of publication | Inorganic chemistry |
Year of publication | 2014 |
Journal volume | 53 |
Journal issue | 3 |
Pages of publication | 1721 - 1728 |
a | 14.7533 ± 0.0011 Å |
b | 21.8439 ± 0.0016 Å |
c | 24.5355 ± 0.0017 Å |
α | 73.335 ± 0.001° |
β | 81.164 ± 0.002° |
γ | 86.668 ± 0.001° |
Cell volume | 7484.2 ± 0.9 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1055 |
Residual factor for significantly intense reflections | 0.0739 |
Weighted residual factors for significantly intense reflections | 0.2047 |
Weighted residual factors for all reflections included in the refinement | 0.2204 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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