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Information card for entry 4337421
Preview
Coordinates | 4337421.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C160.5 H177 N4 O29 P2 W4 |
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Calculated formula | C150.06 H162.125 N3.786 O29.09 P1.998 W4 |
Title of publication | Synthesis, Structure and Cation-Binding Properties of Some [4 + 4] Metallocyclic MO2(2+) (M = Mo or W) Derivatives of 9-Phenyl-2,3,7-trihydroxyfluor-6-one. |
Authors of publication | McCormick, Laura J.; Abrahams, Brendan F.; Boughton, Berin A.; Grannas, Martin J.; Hudson, Timothy A.; Robson, Richard |
Journal of publication | Inorganic chemistry |
Year of publication | 2014 |
Journal volume | 53 |
Journal issue | 3 |
Pages of publication | 1721 - 1728 |
a | 18.4066 ± 0.0004 Å |
b | 20.8649 ± 0.0002 Å |
c | 21.3598 ± 0.0005 Å |
α | 88.312 ± 0.001° |
β | 65.145 ± 0.002° |
γ | 83.726 ± 0.001° |
Cell volume | 7397.6 ± 0.3 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0769 |
Residual factor for significantly intense reflections | 0.0612 |
Weighted residual factors for significantly intense reflections | 0.1869 |
Weighted residual factors for all reflections included in the refinement | 0.1964 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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