Information card for entry 4337451

Structure parameters

• Formula: C26 H34 F I N P Pd S
• Calculated formula: C26 H34 F I N P Pd S
• Title of publication: Room temperature rapid functionalization of E-H bonds (E = O, N, S) via the metal-ligand cooperation mechanism.
• Authors of publication: Scharf, Adam; Goldberg, Israel; Vigalok, Arkadi
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 1
• Pages of publication: 12 - 14
• a: 8.7535 ± 0.0004 Å
• b: 11.5398 ± 0.0005 Å
• c: 15.0375 ± 0.0007 Å
• α: 69.022 ± 0.002°
• β: 77.424 ± 0.002°
• γ: 72.829 ± 0.002°
• Cell volume: 1344.36 ± 0.11 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1387
• Weighted residual factors for all reflections included in the refinement: 0.1473
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No