Information card for entry 4337676

Structure parameters

• Formula: C42 H72 N4 O16 V4
• Calculated formula: C42 H68 N4 O16 V4
• Title of publication: A Novel Octanuclear Vanadium(V) Oxide Cluster Complex Having an Unprecedented Neutral V8O20 Core Functionalized with 4,4'-Di-tert-butyl-2,2'-bipyridine.
• Authors of publication: Kodama, Shintaro; Taya, Nobuto; Ishii, Youichi
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 6
• Pages of publication: 2754 - 2756
• a: 15.487 ± 0.003 Å
• b: 9.647 ± 0.0015 Å
• c: 18.471 ± 0.003 Å
• α: 90°
• β: 107.928 ± 0.0017°
• γ: 90°
• Cell volume: 2625.6 ± 0.8 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for all reflections included in the refinement: 0.1444
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No