Information card for entry 4337695

Structure parameters

• Formula: C34 H60 Cl2 F6 N12 O2 Os2 P
• Calculated formula: C34 H60 Cl2 F6 N12 O2 Os2 P
• Title of publication: Correction to Proof by EPR Spectroscopy that the Unpaired Electron in an Os2(7+) Species Is in a δ* Metal-based Molecular Orbital.
• Authors of publication: Cotton, F. Albert; Chiarella, Gina M.; Dalal, Naresh S.; Murillo, Carlos A.; Wang, Zhenxing; Young, Mark D.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 6
• Pages of publication: 3253
• a: 17.195 ± 0.003 Å
• b: 25.155 ± 0.005 Å
• c: 9.9897 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4320.9 ± 1.4 ų
• Cell temperature: 30 ± 2 K
• Ambient diffraction temperature: 30 ± 2 K
• Number of distinct elements: 8
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.063
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1039
• Weighted residual factors for all reflections included in the refinement: 0.1134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.395
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No