Information card for entry 4337808

Structure parameters

• Formula: C86.27 H64.54 Dy3 N9 O10.76
• Calculated formula: C86.271 H64.542 Dy3 N9 O10.757
• Title of publication: Structure, magnetic behavior, and anisotropy of homoleptic trinuclear lanthanoid 8-quinolinolate complexes.
• Authors of publication: Chilton, Nicholas F.; Deacon, Glen B.; Gazukin, Olga; Junk, Peter C.; Kersting, Berthold; Langley, Stuart K.; Moubaraki, Boujemaa; Murray, Keith S.; Schleife, Frederik; Shome, Mahasish; Turner, David R.; Walker, Julia A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 5
• Pages of publication: 2528 - 2534
• a: 12.313 ± 0.003 Å
• b: 16.612 ± 0.003 Å
• c: 18.099 ± 0.004 Å
• α: 83.78 ± 0.03°
• β: 78.86 ± 0.03°
• γ: 83.49 ± 0.03°
• Cell volume: 3594.6 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0394
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.0952
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No