Information card for entry 4337823

Structure parameters

• Formula: C52 H44 Br2 N4 O2 Os P2
• Calculated formula: C52 H44 Br2 N4 O2 Os P2
• Title of publication: Ruthenium, Rhodium, Osmium, and Iridium Complexes of Osazones (Osazones = Bis-Arylhydrazones of Glyoxal): Radical versus Nonradical States.
• Authors of publication: Patra, Sarat Chandra; Weyhermüller, Thomas; Ghosh, Prasanta
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 5
• Pages of publication: 2427 - 2440
• a: 19.182 ± 0.003 Å
• b: 16.005 ± 0.001 Å
• c: 17.914 ± 0.003 Å
• α: 90°
• β: 113.708 ± 0.012°
• γ: 90°
• Cell volume: 5035.6 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0281
• Residual factor for significantly intense reflections: 0.0245
• Weighted residual factors for significantly intense reflections: 0.0571
• Weighted residual factors for all reflections included in the refinement: 0.0586
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No