Information card for entry 4337859

Structure parameters

• Formula: C74 H84 N8 O24 Tb4
• Calculated formula: C74 H84 N8 O24 Tb4
• Title of publication: Hydroxide-Free Cubane-Shaped Tetranuclear [Ln4] Complexes.
• Authors of publication: Das, Sourav; Dey, Atanu; Biswas, Sourav; Colacio, Enrique; Chandrasekhar, Vadapalli
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3417
• a: 17.781 ± 0.003 Å
• b: 17.155 ± 0.003 Å
• c: 26.846 ± 0.004 Å
• α: 90°
• β: 100.194 ± 0.003°
• γ: 90°
• Cell volume: 8060 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0629
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0911
• Weighted residual factors for all reflections included in the refinement: 0.101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No