Information card for entry 4337867

Structure parameters

• Formula: C48 H80 O32 Pd8 S16
• Calculated formula: C48 H78.5 O32 Pd8 S16
• Title of publication: Tiara-like Octanuclear Palladium(II) and Platinum(II) Thiolates and Their Inclusion Complexes with Dihalo- or Iodoalkanes.
• Authors of publication: Yamashina, Yukari; Kataoka, Yasutaka; Ura, Yasuyuki
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3558
• a: 44.2046 ± 0.0009 Å
• b: 58.0184 ± 0.0014 Å
• c: 13.2016 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 33857.9 ± 1.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0437
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.1021
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No