Information card for entry 4337872

Structure parameters

• Formula: C49 H82 Br2 O32 Pd8 S16
• Calculated formula: C49 H72.75 Br2 O32 Pd8 S16
• Title of publication: Tiara-like Octanuclear Palladium(II) and Platinum(II) Thiolates and Their Inclusion Complexes with Dihalo- or Iodoalkanes.
• Authors of publication: Yamashina, Yukari; Kataoka, Yasutaka; Ura, Yasuyuki
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3558
• a: 44.4317 ± 0.0016 Å
• b: 57.845 ± 0.002 Å
• c: 13.4171 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 34484 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0676
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.1542
• Weighted residual factors for all reflections included in the refinement: 0.167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No