Information card for entry 4337965

Structure parameters

• Formula: C24.5 H48 Cl5 Ga N2 P2
• Calculated formula: C24.5 H48 Cl5 Ga N2 P2
• Title of publication: Azidophosphenium Cations: Versatile Reagents in Inorganic Synthesis.
• Authors of publication: Hering, Christian; Hertrich, Maximilian; Schulz, Axel; Villinger, Alexander
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3880
• a: 19.3622 ± 0.0014 Å
• b: 10.609 ± 0.0009 Å
• c: 32.315 ± 0.002 Å
• α: 90°
• β: 96.085 ± 0.002°
• γ: 90°
• Cell volume: 6600.5 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1328
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1157
• Weighted residual factors for all reflections included in the refinement: 0.1476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No