Information card for entry 4337967

Structure parameters

• Formula: C6 H14 Cl1.21 N3.38 P
• Calculated formula: C6 H14 Cl1.208 N3.376 P
• Title of publication: Azidophosphenium Cations: Versatile Reagents in Inorganic Synthesis.
• Authors of publication: Hering, Christian; Hertrich, Maximilian; Schulz, Axel; Villinger, Alexander
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 7
• Pages of publication: 3880
• a: 6.3996 ± 0.0005 Å
• b: 11.0092 ± 0.0009 Å
• c: 7.7964 ± 0.0006 Å
• α: 90°
• β: 98.145 ± 0.004°
• γ: 90°
• Cell volume: 543.75 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0835
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No