Information card for entry 4338269

Structure parameters

• Formula: C125 H256 N14 O27 Tb4
• Calculated formula: C125 H256 N14 O27 Tb4
• Title of publication: Preparation of n,n-dialkylcarbamato lanthanide complexes by extraction of lanthanide ions from aqueous solution into hydrocarbons.
• Authors of publication: Armelao, Lidia; Belli Dell'Amico, Daniela; Biagini, Paolo; Bottaro, Gregorio; Chiaberge, Stefano; Falvo, Paola; Labella, Luca; Marchetti, Fabio; Samaritani, Simona
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 10
• Pages of publication: 4861 - 4871
• a: 31.399 ± 0.006 Å
• b: 27.759 ± 0.005 Å
• c: 17.295 ± 0.003 Å
• α: 90°
• β: 92.963 ± 0.002°
• γ: 90°
• Cell volume: 15054 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2179
• Residual factor for significantly intense reflections: 0.1186
• Weighted residual factors for significantly intense reflections: 0.2909
• Weighted residual factors for all reflections included in the refinement: 0.3472
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No