Information card for entry 4338348

Structure parameters

• Formula: C73 H73 B F24 N4 O2 Rh
• Calculated formula: C73 H73 B F24 N4 O2 Rh
• Title of publication: 1,2-Addition of Dihydrogen across Rhodium(III)-OMe Bonds.
• Authors of publication: Burgess, Samantha A.; Devarajan, Deepa; Bolaño, Tamara; Ess, Daniel H.; Gunnoe, T. Brent; Sabat, Michal; Myers, William H.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 10
• Pages of publication: 5328 - 5340
• a: 12.0942 ± 0.0004 Å
• b: 19.064 ± 0.0006 Å
• c: 19.0652 ± 0.0006 Å
• α: 113.54 ± 0.001°
• β: 91.283 ± 0.001°
• γ: 107.721 ± 0.001°
• Cell volume: 3786.2 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0516
• Weighted residual factors for significantly intense reflections: 0.1385
• Weighted residual factors for all reflections included in the refinement: 0.1401
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No