Crystallography Open Database

Information card for entry 4338354

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Coordinates	4338354.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C110 H82 Gd10 O56 S22
Calculated formula	C110.008 H82.006 Gd10 O56 S22.002
Title of publication	An unprecedented decanuclear Gd(III) cluster for magnetic refrigeration.
Authors of publication	Liu, Sui-Jun; Zhao, Jiong-Peng; Tao, Jun; Jia, Ji-Min; Han, Song-De; Li, Yue; Chen, Yan-Cong; Bu, Xian-He
Journal of publication	Inorganic chemistry
Year of publication	2013
Journal volume	52
Journal issue	16
Pages of publication	9163 - 9165
a	14.333 ± 0.004 Å
b	15.442 ± 0.004 Å
c	17.03 ± 0.005 Å
α	70.703 ± 0.011°
β	87.221 ± 0.016°
γ	75.803 ± 0.015°
Cell volume	3446.7 ± 1.7 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0637
Residual factor for significantly intense reflections	0.0429
Weighted residual factors for significantly intense reflections	0.0732
Weighted residual factors for all reflections included in the refinement	0.0809
Goodness-of-fit parameter for all reflections included in the refinement	0.915
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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