Information card for entry 4338364

Structure parameters

• Formula: C66 H0 N4 O40 Si V2 W10
• Calculated formula: C66 N4 O40 Si V2 W10
• Title of publication: Amphiprotic Properties of a Bis(μ-hydroxo)divanadium(IV)-Substituted γ-Keggin-Type Silicodecatungstate Containing Two Different Kinds of Hydroxyl Moieties.
• Authors of publication: Uehara, Kazuhiro; Miyachi, Takuya; Mizuno, Noritaka
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 10
• Pages of publication: 5341 - 5347
• a: 24.6843 ± 0.0004 Å
• b: 25.0863 ± 0.0005 Å
• c: 17.2103 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10657.3 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.2354
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No